Inventors:
NICHOLAS J. CONDON - Greenbelt MD, US
Steven R. Bowman - Edgewater MD, US
Shawn P. O'Connor - Dunkirk VA, US
International Classification:
C30B 11/02
Abstract:
A method and apparatus for growing a single crystal KbClmaterial in a growth furnace comprising an upper zone set at 480° C. A single crystal KbClmaterial is grown from a single KbClgrain until a eutectic point is reached. The upper zone is cooled at 1°/hour to 380° C. The single crystal KbClmaterial is annealed. The single crystal KbClmaterial is cooled at 10°/hour to room temperature. Optionally, the method further includes loading an ampoule with KbClpowder, the ampoule including a plug, which includes a seeding well and an aperture. The KbClpowder is melted, thereby generating a melt. The melt is frozen to capture a polycrystalline KbClmaterial in the seeding well, thereby generating a polycrystalline KbClseed. The ampoule is loaded into the growth furnace. The polycrystalline KbClmaterial is melted except for the polycrystalline KbClseed, the polycrystalline KbClseed including the single KbClgrain. The polycrystalline KbClmaterial is grown until the single KbClgrain is isolated by the aperture.