Inventors:
Murray Katz - Newington CT
Arthur Kaufman - Bloomfield CT
Assignee:
Union Technologies Corporation - East Hartford CT
International Classification:
H01M 486, H01M 488
Abstract:
A porous conducting particle, hydrophobic bonded, substrate supported electrode is prewetted with the electrolyte. A D. C. voltage is applied to the electrode to assist in the prewetting with the electrolyte. A soluble catalyst-containing material is then introduced into the electrode and the catalyst deposited within the electrode. By appropriate selection of the porous conducting particles and the catalyst-applying techniques, precise control of the location of the catalyst can be obtained. If graphite materials are used as the conducting particles, a catalyst-containing salt is allowed to dissolve in the electrolyte in the prewetted electrode, and the catalyst-containing material is reduced to the metal. If the reduction is done by reaction with a reducing gas such as hydrogen, the catalyst will be deposited only in those regions of the electrode at which there is an electrolyte-reactant gas interface which is in electrical-conducting relationship with the substrate. Alternatively, extremely precise amounts of catalyst can be deposited within the electrode structure by use of a solution of a compound of the catalyst whose wettability with the hydrophobic material varies as the solution evaporates.