Inventors:
James Joseph Downs - Kingsport TN
Andrew Charles Hiester - Kingsport TN
Mark Elliott Taylor - Orange TX
Mark Allan Mueller - Austin TX
Michael Warren Peters - Gilbert AZ
William Pleasie Nelson - Nederland TX
Assignee:
Huntsman Specialty Chemicals Corp. - Austin TX
International Classification:
B01D 340, B01D 342, C07D30132
Abstract:
In the continuous purification of a propylene oxide feedstock contaminated with water, methanol and acetone wherein an acetone buffer is established in the column, normal distillation conditions are maintained or restored during or after an upset by continuously monitoring predetermined distillation conditions in the acetone buffer zone, and adding additional acetone to the extractive distillation column when the monitored distillation condition deviates from a predetermined value by a predetermined amount.