Inventors:
George J. Hudak - Kennett Square PA
Assignee:
Hewlett-Packard Company - Palo Alto CA
International Classification:
H05B 666
Abstract:
A system for monitoring the progress of a chemical reaction in a microwave-assisted preparation of a sample, having a microwave energy source, a waveguide coupled to the microwave energy source and having a waveguide cavity, and a resistive load coupled to the waveguide, wherein the sample that is to be subject to microwave-assisted heating is situated in a reaction vessel. The reaction vessel is located in the path of the forward microwave radiation between the microwave energy source and the resistive load. An energy monitoring device is interposed between the reaction vessel and the resistive load so as to monitor the energy not absorbed by the reaction vessel. The energy absorbed by the sample may be calculated in accordance with the level of energy measured by the energy monitoring device to provide a value that indicates the status of the chemical reaction. Alternatively, the reaction vessel may be located in the path of the forward microwave radiation between the microwave energy source and a terminal end of the waveguide. An isolator provided in the form of a circulator coupled to the resistive load is located in the path of the forward microwave radiation between the microwave energy source and the reaction vessel so as to allow the forward energy to proceed to the sample, and to divert reverse energy to the resistive load.